{"id":127743,"date":"2023-10-23T14:15:10","date_gmt":"2023-10-23T06:15:10","guid":{"rendered":"https:\/\/keidy.com.tw\/?p=127743"},"modified":"2023-11-30T17:54:20","modified_gmt":"2023-11-30T09:54:20","slug":"tbn%e7%b8%bd%e9%b9%bc%e5%83%b9%e6%bb%b4%e5%ae%9a%e5%88%86%e6%9e%90","status":"publish","type":"post","link":"https:\/\/keidy.com.tw\/tbn%e7%b8%bd%e9%b9%bc%e5%83%b9%e6%bb%b4%e5%ae%9a%e5%88%86%e6%9e%90\/","title":{"rendered":"\u7e3d\u9e7c\u50f9TBN\u6ef4\u5b9a\u5206\u6790"},"content":{"rendered":"\t\t
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\u6839\u64daASTM D2896\/ISO 3771\u6e2c\u5b9a\u7e3d\u9e7c\u50f9<\/h2>\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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\u27a4 \u6982\u8ff0<\/h2>\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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\u4ee5\u9ad8\u6c2f\u9178\u6eb6\u65bc\u51b0\u918b\u9178\u7684\u6eb6\u6db2\u9032\u884c\u96fb\u4f4d\u6ef4\u5b9a\u6e2c\u5b9a\u77f3\u6cb9\u7522\u54c1\u7684\u57fa\u672c\u6210\u4efd\u3002\u7e3d\u9e7c\u503c (TBN) \u662f\u4e2d\u548c 1 g \u4e2d\u542b\u6709\u7684\u6240\u6709\u9e7c\u6027\u6210\u4efd\u6240\u9700\u7684\u9ad8\u6c2f\u9178\u7684\u91cf\uff0c\u4ee5\u6c2b\u6c27\u5316\u9240\u7684\u6beb\u514b\u7576\u91cf\uff08\u6216\u6bcf\u514b\u6c2b\u6c27\u5316\u9240\u7684\u6beb\u514b\u7576\u91cf\uff09\u8868\u793a\u3002 \u5728\u898f\u5b9a\u7684\u689d\u4ef6\u4e0b\u6ef4\u5b9a\u6a23\u54c1\u7684\u91cf\u3002<\/span><\/p>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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\u27a4 \u672c\u6e2c\u5b9a\u4e2d\u4f7f\u7528\u7684\u5100\u5668\u53ca\u8a66\u5291<\/h2>\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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\u5100\u5668\u8207\u914d\u5099<\/strong><\/span><\/p>
\u81ea\u52d5\u6ef4\u5b9a\u5100<\/td>TitroLine 7000 with 10 ml unit<\/td><\/tr>
\u6ef4\u5b9a\u982d<\/td>TZ 1643<\/td><\/tr>
\u96fb\u6975<\/td>M 6480 eth<\/td><\/tr>
\u96fb\u6975\u586b\u5145\u6db2<\/td>LiCl\/ethanol, L 503 4<\/td><\/tr>
\u652a\u62cc\u5668<\/td>TM 235<\/td><\/tr>
\u5176\u4ed6\u914d\u5099<\/td>\u5370\u8868\u6a5f, USB\u6216TitriSoft\u8edf\u9ad4<\/td><\/tr><\/tbody><\/table>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t
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\u8a66\u5291<\/strong><\/span><\/p>
1.<\/td>\u6eb6\u5291: \u51b0\u918b\u9178\/\u6c2f\u82ef (1\/2)<\/td><\/tr>
2.<\/td>\u6a19\u6e96\u6db2:\u542b\u9130\u82ef\u4e8c\u7532\u9178\u6c2b\u9240 (KHC8H4O4) \u6216\u201cTris\u201d<\/td><\/tr>
3.<\/td>\u6ef4\u5b9a\u6db2:0.1 mol\/L\u9ad8\u6c2f\u9178\u6eb6\u65bc\u51b0\u918b\u9178\u6eb6\u6db2<\/td><\/tr><\/tbody><\/table>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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\u27a4 \u6ef4\u5b9a\u7a0b\u5e8f<\/h2>\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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\u9ad8\u6c2f\u9178\u6eb6\u6db2\u7684\u88fd\u5099<\/strong><\/span><\/p>

\u8acb\u4f7f\u7528\u201c\u5373\u7528\u578b\u201d\u6ef4\u5b9a\u6eb6\u6db2 0.1 mol\/L\u3002<\/span><\/p>

\u6a19\u6e96\u5316<\/strong><\/span><\/p>

\u9130\u82ef\u4e8c\u7532\u9178\u6c2b\u9240\u5fc5\u9808\u5728\u70d8\u7bb1\uff08110-120\u00b0C\uff09\u4e2d\u4e7e\u71e5\uff0c\u7136\u5f8c\u5728\u4e7e\u71e5\u5668\u4e2d\u51b7\u537b\u3002\u00a0<\/span><\/p>

\u53d60.15\uff5e0.2g\u9130\u82ef\u4e8c\u7532\u9178\u6c2b\u9240\u6216Tris\uff0c\u7cbe\u78ba\u81f30.1mg\uff0c\u52a0\u71b1\u6eb6\u89e3\u65bc40ml\u4e59\u9178\u4e2d\u3002 \u6dfb\u52a080\u6beb\u5347\u6c2f\u82ef\u3002 \u4f7f\u7528\u65b9\u6cd5->\u6ef4\u5ea6\u9ad8\u6c2f\u9178\u3002 \u91cd\u8907\u6a19\u6e96\u53163\u6b21\uff0c\u5176\u5e73\u5747\u503c\u81ea\u52d5\u5b58\u5132\u5728\u667a\u6167\u578b\u6ef4\u5b9a\u7ba1\u4e2d\u3002<\/span><\/p>

\u00a0<\/p>

\u6eb6\u5291\u6df7\u5408\u7684\u7a7a\u767d\u503c<\/strong><\/span><\/p>

\u5c07120mL\u7684\u6ef4\u5b9a\u6eb6\u6db2\u6dfb\u52a0\u81f3\u71d2\u676f\u4e2d\uff0c\u5c07\u71d2\u676f\u653e\u7f6e\u5728\u96fb\u78c1\u652a\u62cc\u5668\u5f8c\u958b\u59cb\u6ef4\u5b9a\u65b9\u6cd5\u3002\u5728\u6ef4\u5b9a\u5f8c\uff0c\u4f7f\u7528\u6eb6\u5291\u6e05\u6d17\u96fb\u6975\u53ca\u6ef4\u5b9a\u7ba1\u5c16\u7aef\uff0c\u7136\u5f8c\u7528\u6c34\u6c96\u6d17\uff0c\u7136\u5f8c\u518d\u6b21\u7528\u6eb6\u5291\u6c96\u6d17\u71d2\u676f\u7d04 1 \u5206\u9418\u3002<\/span><\/p>

\u4f7f\u7528\u65b9\u6cd5 BLANK_TBN<\/span><\/p>

\u91cd\u8907\u7a7a\u767d\u6ef4\u5b9a\u4e00\u6b21\u3002 \u5e73\u5747\u503c\u53ef\u4ee5\u5132\u5b58\u5728\u5168\u5c40\u5b58\u5132\u5668\u4e2d\uff0c\u4f8b\u5982 M01\uff08TBN\u7a7a\u767d\uff09\u5fc5\u9808\u9810\u5148\u5efa\u7acb\u3002<\/span><\/p>

\u00a0<\/p>

\u6a23\u54c1\u6ef4\u5b9a<\/strong><\/span><\/p>

\u6839\u64da\u9810\u671f\u7e3d\u9e7c\u503c (TBN) \u8a08\u7b97\u6240\u9700\u6a23\u54c1\u7684\u6578\u91cf<\/span><\/p>

\u516c\u5f0f\u5982\u4e0b\uff1a<\/span><\/p>

\u00a0<\/p>
\u00a0<\/span>
\u00a0<\/span><\/td>		\u6a23\u54c1\u7684\u8fd1\u4f3c\u8cea\u91cf<\/span>
\uff08\u4ee5\u514b\u70ba\u55ae\u4f4d\uff09<\/span><\/td>		=<\/span><\/td>28<\/span><\/td>\u00a0<\/td><\/tr>
\u9810\u671f TBN<\/span><\/td><\/tr><\/tbody><\/table>

\u00a0<\/p>

\u5728 250 mL \u71d2\u676f\u4e2d\u79e4\u91cf\u6a23\u54c1\uff0c\u4e26\u6dfb\u52a0 120 ml\u6ef4\u5b9a\u6eb6\u5291\u81f3\u6a23\u54c1\u4e2d\u3002 \u5c07\u71d2\u676f\u653e\u5728\u96fb\u78c1\u652a\u62cc\u5668\u4e0a\u4e26\u958b\u59cb\u6ef4\u5b9a\u65b9\u6cd5\u3002 \u6ef4\u5b9a\u5f8c\uff0c\u7528\u6eb6\u5291\u6c96\u6d17\u96fb\u6975\u548c\u6ef4\u5b9a\u7ba1\u5c16\u7aef\uff0c\u7136\u5f8c\u7528\u6c34\u6c96\u6d17\uff0c\u7136\u5f8c\u518d\u6b21\u7528\u71d2\u676f\u4e2d\u7684\u6eb6\u5291\u6c96\u6d17\u7d04 1 \u5206\u9418\u3002 \u4f7f\u7528 TBN ISO ASTM \u65b9\u6cd5\u3002<\/span><\/p>

\u96fb\u6975\u7684\u7dad\u8b77<\/strong><\/span><\/p>

\u5982\u679c\u60a8\u4f7f\u7528 N 6480 \u7b49\u8907\u5408\u96fb\u6975\uff0c\u8acb\u5c07\u96fb\u6975\u5b58\u653e\u5728 LiCl\/\u51b0\u918b\u9178\u96fb\u89e3\u6db2\u4e2d<\/span><\/p>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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\n\t\t\t\t\t\t\t\t\t\t\t\t\t\"\"\t\t\t\t\t\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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Method data<\/td><\/tr>
Method name:<\/td>Blank TBN 2896<\/td>Titration duration:<\/td>5 m 11 s<\/td><\/tr>
Method type:<\/td>Automatic titration<\/td>Damping settings:<\/td>strong<\/td><\/tr>
Measured value:<\/td>mV<\/td>Documentation:<\/td>GLP<\/td><\/tr>
Titration mode:<\/td>Linear<\/td>Measuring speed \/ drift<\/td>10s<\/td><\/tr>
Initial waiting time:<\/td>10 s<\/td>Titration direction:<\/td>Increase<\/td><\/tr>
Pretitration:<\/td>Off<\/td>End value:<\/td>Off<\/td><\/tr>
EQ:<\/td>On (1)<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
Slope value:<\/td>Flat<\/td>Value\u0001<\/td>120\u0001<\/td><\/tr>
Titration data<\/td><\/tr>
Sample ID:<\/td>blank 1<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
Start mV:<\/td>533.2 mV<\/td>End mV:<\/td>704.6 mV<\/td><\/tr>
EQ:<\/td>0.02 ml \/ 610.1 mV<\/td>Blank:<\/td>0.02 ml<\/td><\/tr>
Dosing parameter<\/td><\/tr>
Dosing speed:<\/td>100 %<\/td>Filling speed<\/td>30 s<\/td><\/tr>
Maximum dosing volume:<\/td>15.00 ml<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
Calculation formula<\/td><\/tr>
Blank:<\/td>EQ-> M02<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
Statistics:<\/td>Off<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
Unit values<\/td><\/tr>
Unit size:<\/td>20 ml<\/td>Reagent:<\/td>HCl04 0.1 mol\/L<\/td><\/tr>
Concentration:<\/td>0.10150mol\/l<\/td>\u00a0<\/td>\u00a0<\/td><\/tr><\/tbody><\/table>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t<\/div>\n\t\t","protected":false},"excerpt":{"rendered":"

\u6839\u64daASTM D2896\/ISO 3771\u6e2c\u5b9a\u7e3d\u9e7c\u50f9 \u27a4 \u6982\u8ff0 \u4ee5\u9ad8\u6c2f\u9178\u6eb6\u65bc\u51b0\u918b\u9178\u7684\u6eb6\u6db2\u9032\u884c\u96fb\u4f4d\u6ef4\u5b9a\u6e2c\u5b9a\u77f3\u6cb9\u7522 […]<\/p>\n","protected":false},"author":9,"featured_media":127444,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"ocean_post_layout":"","ocean_both_sidebars_style":"","ocean_both_sidebars_content_width":0,"ocean_both_sidebars_sidebars_width":0,"ocean_sidebar":"0","ocean_second_sidebar":"0","ocean_disable_margins":"enable","ocean_add_body_class":"","ocean_shortcode_before_top_bar":"","ocean_shortcode_after_top_bar":"","ocean_shortcode_before_header":"","ocean_shortcode_after_header":"","ocean_has_shortcode":"","ocean_shortcode_after_title":"","ocean_shortcode_before_footer_widgets":"","ocean_shortcode_after_footer_widgets":"","ocean_shortcode_before_footer_bottom":"","ocean_shortcode_after_footer_bottom":"","ocean_display_top_bar":"default","ocean_display_header":"default","ocean_header_style":"","ocean_center_header_left_menu":"0","ocean_custom_header_template":"0","ocean_custom_logo":0,"ocean_custom_retina_logo":0,"ocean_custom_logo_max_width":0,"ocean_custom_logo_tablet_max_width":0,"ocean_custom_logo_mobile_max_width":0,"ocean_custom_logo_max_height":0,"ocean_custom_logo_tablet_max_height":0,"ocean_custom_logo_mobile_max_height":0,"ocean_header_custom_menu":"0","ocean_menu_typo_font_family":"0","ocean_menu_typo_font_subset":"","ocean_menu_typo_font_size":0,"ocean_menu_typo_font_size_tablet":0,"ocean_menu_typo_font_size_mobile":0,"ocean_menu_typo_font_size_unit":"px","ocean_menu_typo_font_weight":"","ocean_menu_typo_font_weight_tablet":"","ocean_menu_typo_font_weight_mobile":"","ocean_menu_typo_transform":"","ocean_menu_typo_transform_tablet":"","ocean_menu_typo_transform_mobile":"","ocean_menu_typo_line_height":0,"ocean_menu_typo_line_height_tablet":0,"ocean_menu_typo_line_height_mobile":0,"ocean_menu_typo_line_height_unit":"","ocean_menu_typo_spacing":0,"ocean_menu_typo_spacing_tablet":0,"ocean_menu_typo_spacing_mobile":0,"ocean_menu_typo_spacing_unit":"","ocean_menu_link_color":"","ocean_menu_link_color_hover":"","ocean_menu_link_color_active":"","ocean_menu_link_background":"","ocean_menu_link_hover_background":"","ocean_menu_link_active_background":"","ocean_menu_social_links_bg":"","ocean_menu_social_hover_links_bg":"","ocean_menu_social_links_color":"","ocean_menu_social_hover_links_color":"","ocean_disable_title":"default","ocean_disable_heading":"default","ocean_post_title":"","ocean_post_subheading":"","ocean_post_title_style":"","ocean_post_title_background_color":"","ocean_post_title_background":0,"ocean_post_title_bg_image_position":"","ocean_post_title_bg_image_attachment":"","ocean_post_title_bg_image_repeat":"","ocean_post_title_bg_image_size":"","ocean_post_title_height":0,"ocean_post_title_bg_overlay":0.5,"ocean_post_title_bg_overlay_color":"","ocean_disable_breadcrumbs":"default","ocean_breadcrumbs_color":"","ocean_breadcrumbs_separator_color":"","ocean_breadcrumbs_links_color":"","ocean_breadcrumbs_links_hover_color":"","ocean_display_footer_widgets":"default","ocean_display_footer_bottom":"default","ocean_custom_footer_template":"0","footnotes":"","ocean_post_oembed":"","ocean_post_self_hosted_media":"","ocean_post_video_embed":"","ocean_link_format":"","ocean_link_format_target":"self","ocean_quote_format":"","ocean_quote_format_link":"post","ocean_gallery_link_images":"on","ocean_gallery_id":[]},"categories":[1997],"tags":[],"_links":{"self":[{"href":"https:\/\/keidy.com.tw\/wp-json\/wp\/v2\/posts\/127743"}],"collection":[{"href":"https:\/\/keidy.com.tw\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/keidy.com.tw\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/keidy.com.tw\/wp-json\/wp\/v2\/users\/9"}],"replies":[{"embeddable":true,"href":"https:\/\/keidy.com.tw\/wp-json\/wp\/v2\/comments?post=127743"}],"version-history":[{"count":1,"href":"https:\/\/keidy.com.tw\/wp-json\/wp\/v2\/posts\/127743\/revisions"}],"predecessor-version":[{"id":127767,"href":"https:\/\/keidy.com.tw\/wp-json\/wp\/v2\/posts\/127743\/revisions\/127767"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/keidy.com.tw\/wp-json\/wp\/v2\/media\/127444"}],"wp:attachment":[{"href":"https:\/\/keidy.com.tw\/wp-json\/wp\/v2\/media?parent=127743"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/keidy.com.tw\/wp-json\/wp\/v2\/categories?post=127743"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/keidy.com.tw\/wp-json\/wp\/v2\/tags?post=127743"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}