{"id":127826,"date":"2023-11-28T16:30:53","date_gmt":"2023-11-28T08:30:53","guid":{"rendered":"https:\/\/keidy.com.tw\/?p=127826"},"modified":"2023-11-30T16:24:01","modified_gmt":"2023-11-30T08:24:01","slug":"%e7%b8%bd%e9%85%b8%e5%83%b9tan%e6%bb%b4%e5%ae%9a%e5%88%86%e6%9e%90-astm-d664","status":"publish","type":"post","link":"https:\/\/keidy.com.tw\/%e7%b8%bd%e9%85%b8%e5%83%b9tan%e6%bb%b4%e5%ae%9a%e5%88%86%e6%9e%90-astm-d664\/","title":{"rendered":"\u7e3d\u9178\u50f9TAN\u6ef4\u5b9a\u5206\u6790-ASTM D664"},"content":{"rendered":"\t\t
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\u81ea\u52d5\u6ef4\u5b9a<\/span><\/h2>\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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\u4ee5\u96fb\u4f4d\u6ef4\u5b9a\u6cd5\u6e2c\u5b9a\u77f3\u6cb9\u7522\u54c1\u548c\u6f64\u6ed1\u5291\u4e2d\u7684\u9178\u6027\u5316\u5408\u7269\u3002\u7e3d\u9178\u50f9TAN\u662f\u4e2d\u548c1g\u6a23\u54c1\u4e2d\u6240\u6709\u9178\u6027\u6210\u5206\u6240\u9700\u7684\u9e7c\u91cf\uff0c\u4ee5NaOH\u6beb\u514b\u6578\u8868\u793a\u3002\u6ef4\u5b9a\u5728\u7532\u82ef\u3001\u7570\u4e19\u9187\u548c\u6c34\u7684\u6df7\u5408\u7269\u4e2d\u4ee5\u53ca\u7570\u4e19\u9187\u4e2d\u7684 KOH \u4e2d\u9032\u884c\u6e2c\u5b9a\u4e5f\u53ef\u4ee5\u4f7f\u7528\u6c2b\u6c27\u5316\u56db\u4e01\u57fa\u92a8\u4f5c\u70ba\u6ef4\u5b9a\u5291\uff0c\u7d50\u679c\u4ee5mg(KOH)\/g\u8a08\u7b97\u3002<\/span><\/p>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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\u5100\u5668\u8207\u914d\u5099<\/strong><\/span><\/p>
\u81ea\u52d5\u6ef4\u5b9a\u5100<\/td>TL 7000 \u6216\u66f4\u9ad8\u968e<\/td><\/tr>
\u96fb\u6975<\/td>M 6480 eth<\/td><\/tr>
\u96fb\u6975\u7dda<\/td>L 1 A<\/td><\/tr>
\u53c3\u8003\u96fb\u6975<\/td>B 2920+<\/td><\/tr>
\u96fb\u6975\u7dda<\/td>L 1 N<\/td><\/tr>
\u652a\u62cc\u5668<\/td>TM 235<\/td><\/tr>
\u5176\u4ed6\u914d\u5099<\/td>150ml\u71d2\u676f\u8868\u9762\u76bf, 30mm, \u78c1\u529b\u652a\u62cc\u68d2<\/td><\/tr><\/tbody><\/table>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t
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\u8a66\u5291<\/strong><\/span><\/p>

\u6240\u6709\u8a66\u5291\u61c9\u70ba\u5206\u6790\u7d1a\u6216\u66f4\u9ad8\u7d1a<\/p>
1.<\/td>KOH 0,1 mol\/l \u4ee5\u7570\u4e19\u9187\u70ba\u6eb6\u5291<\/td><\/tr>
2.<\/td>\u7532\u82ef<\/td><\/tr>
3.<\/td>\u7570\u4e19\u9187<\/td><\/tr>
4.<\/td>\u84b8\u993e\u6c34<\/td><\/tr><\/tbody><\/table>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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\u27a4 \u6ef4\u5b9a\u7a0b\u5e8f<\/h1>\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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\u8a66\u5291<\/strong><\/p>

KOH in Isopropyl alcohol 0.1 mol\/l<\/strong>
\u5efa\u8b70\u4f7f\u7528\u73fe\u6210\u7684 0.1 mol\/l \u6eb6\u6db2\u3002\u5fc5\u9808\u4f7f\u7528\u9209\u77f3\u7070\u7b49\u4e8c\u6c27\u5316\u78b3\u5438\u6536\u5291\u4f86\u4fdd\u8b77\u8a72\u6eb6\u6db2\u514d\u53d7\u4e8c\u6c27\u5316\u78b3\u7684\u5f71\u97ff\u3002 \u6ef4\u5ea6\u6e2c\u5b9a\u6309\u7167\u61c9\u7528\u8aaa\u660e\u201cTiter KOH\u201d\u4e2d\u7684\u63cf\u8ff0\u9032\u884c\u3002<\/p>

\u6eb6\u5291\u6df7\u5408\u7269<\/strong>
\u5c07 500 \u6beb\u5347\u7532\u82ef\u3001495 \u6beb\u5347\u7570\u4e19\u9187\u548c 5 \u6beb\u5347\u6c34\u5728\u74f6\u4e2d\u6df7\u5408\u3002<\/p>

\u96fb\u6975\u7684\u6e05\u6f54<\/strong>
\u9700\u8981\u57f7\u884c 3 \u500b\u6b65\u9a5f\u5c0d\u96fb\u6975\u9032\u884c\u6e05\u6f54\u548c\u8abf\u7bc0<\/p>

  1. \u9996\u5148\u7528\u6eb6\u5291\u6df7\u5408\u7269\u6c96\u6d17\u96fb\u6975\u4ee5\u53bb\u9664\u6a23\u54c1\u6b98\u7559\u7269\u3002\u7136\u5f8c\u5c07\u5176\u5728\u6c34\u4e2d\u9032\u884c\u8abf\u7bc0\u3002<\/li>
  2. \u8abf\u7bc0\u5f8c\uff0c\u7528\u6eb6\u5291\u6df7\u5408\u7269\u6c96\u6d17\u96fb\u6975\u4ee5\u9664\u53bb\u6c34\u3002<\/li>
  3. \u5c07\u96fb\u6975\u5132\u5b58\u5728 1.5 mol\/l LiCl \u7684\u4e59\u9187\u6eb6\u6db2\u4e2d\uff08\u6216\u8005\uff0c\u5982\u679c\u4f7f\u7528\u5176\u4ed6\u96fb\u89e3\u8cea\uff0c\u5247\u5132\u5b58\u5728\u8a72\u96fb\u89e3\u8cea\u6eb6\u6db2\u4e2d\uff09\u3002<\/li><\/ol>

    \u7a7a\u767d\u503c<\/strong>
    \u5c0d\u65bc\u7a7a\u767d\u6ef4\u5b9a\uff0c\u5c07 125 ml \u6eb6\u5291\u653e\u5165 250 ml \u71d2\u676f\u4e2d\uff0c\u4e26\u7528 0.1 mol\/l KOH \u6ef4\u5b9a\u3002 \u7a7a\u767d\u61c9\u4f4e\u65bc 0.3 ml\u3002<\/p>

    \u6a23\u54c1\u88fd\u5099<\/strong>
    \u5c07\u6a23\u54c1\u7a31\u91cd\u653e\u5165 250 ml \u71d2\u676f\u4e2d\uff0c\u6eb6\u89e3\u5728 125 ml \u6eb6\u5291\u4e2d\uff0c\u4e26\u7528 0.1 mol\/l KOH \u6ef4\u5b9a\u3002 \u7531\u65bc\u6ef4\u5b9a\u6642\u9593\u8f03\u9577\uff0c\u61c9\u8a08\u7b97\u6a23\u54c1\u91cd\u91cf\u4e26\u9078\u64c7\u6ef4\u5b9a\u91cf\u4e0d\u8d85\u904e4-5ml\u3002<\/p>

    \u53ef\u4ee5\u6839\u64da\u4ee5\u4e0b\u7d93\u9a57\u6cd5\u5247\u4f30\u8a08\u6240\u9700\u7684\u6a23\u672c\u91cf\uff1a<\/p>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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    \u00a0<\/td>20<\/td>\u00a0<\/td><\/tr>
    W(g)=<\/td>_____________<\/td>\u00a0<\/td><\/tr>
    \u00a0<\/td>\u9810\u671f \ud835\udc47\ud835\udc34\ud835\udc41<\/td><\/tr><\/tbody><\/table>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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    \u27a4 \u6ef4\u5b9a\u53c3\u6578<\/h1>\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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    \n\t\t\t\t\t\t\t\t\t\t\t\t\t\"\"\t\t\t\t\t\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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    Method data<\/td><\/tr>
    Default method:<\/td>Blank TAN-TBN<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
    Method type:<\/td>Automatic titration<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
    Modus:<\/td>linear<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
    Measured value:<\/td>mV<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
    Measuring speed \/ drift:<\/td>User defined<\/td>Fixed delax time<\/span><\/td>12s<\/td><\/tr>
    Initial waiting time:<\/td>10 s<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
    Linear steps:<\/td>0.01ml<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
    Damping:<\/td>strong<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
    Pretitration:<\/td>off<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
    End value:<\/td>off<\/td>Titration direction:<\/td>decrease<\/td><\/tr>
    EQ:<\/td>On(1)<\/td>Delay time:<\/td>0 s<\/td><\/tr>
    Max. titration volume:<\/td>10mL<\/td>Slope value<\/td>60<\/td><\/tr>
    Dosing speed:<\/td>100 %<\/td>Filling speed<\/td>30 s<\/td><\/tr><\/tbody><\/table>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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    \u8a08\u7b97:\u00a0<\/p>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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     \ud835\udc5a\ud835\udc59 = \ud835\udc38\ud835\udc441<\/h3>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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    \n\t\t\t\t\t\t\t\t\t\t\t\t\t\"\"\t\t\t\t\t\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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    Method data<\/td><\/tr>
    Default method:<\/td>TAN ASTM 664<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
    Method type:<\/td>Automatic titration<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
    Modus:<\/td>linear<\/td>Minimum holding time:<\/td>\u00a07s<\/td><\/tr>
    Measured value:<\/td>mV<\/td>Maximum holding time<\/td>\u00a020s<\/td><\/tr>
    Measuring speed \/ drift:<\/td>User defined<\/td>Measuring time<\/td>4s<\/td><\/tr>
    Initial waiting time:<\/td>10 s<\/td>\u00a0Drift<\/td>\u00a010mV\/min<\/td><\/tr>
    Linear steps:<\/td>0.05ml<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
    Damping:<\/td>strong<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
    Pretitration:<\/td>off<\/td>\u00a0<\/td>\u00a0<\/td><\/tr>
    End value:<\/td>off<\/td>Titration direction:<\/td>decrease<\/td><\/tr>
    EQ:<\/td>On(1)<\/td>Delay time:<\/td>0 s<\/td><\/tr>
    Max. titration volume:<\/td>6 mL<\/td>Slope value<\/td>120<\/td><\/tr>
    Dosing speed:<\/td>100 %<\/td>Filling speed<\/td>30 s<\/td><\/tr><\/tbody><\/table>

    \u5c0d\u65bc TAN \u503c\u975e\u5e38\u4f4e\u7684\u6a23\u54c1\uff0c\u7dda\u6027\u6b65\u9032\u53ef\u6e1b\u5c11\u81f3 0.02 \u6216 0.01 ml\u3002<\/p>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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    \u8a08\u7b97:\u00a0<\/p>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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    \u00a0<\/td>(\ud835\udc38\ud835\udc441 \u2212 \ud835\udc35) \u2217 \ud835\udc47 \u2217 \ud835\udc40 \u2217 \ud835\udc391<\/td><\/tr>

    \ud835\udc47\ud835\udc34\ud835\udc41 [\ud835\udc5a\ud835\udc54(\ud835\udc3e\ud835\udc42\ud835\udc3b)\/\ud835\udc54] =<\/p><\/td>

    		——————————–<\/td><\/tr>
    \u00a0<\/td>\ud835\udc4a \u2217 \ud835\udc392<\/td><\/tr><\/tbody><\/table>

    \u00a0<\/p>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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    B<\/td>M01<\/td>Blank value, saved in global Memory M01<\/td><\/tr>
    EQ1<\/td>\u00a0<\/td>Consumption of titrant at first Equivalence point<\/td><\/tr>
    T<\/td>WA<\/td>Concentration of the titrant<\/td><\/tr>
    M<\/td>56,11<\/td>Molecular mass<\/td><\/tr>
    W<\/td>man<\/td>Weight of the sample in g<\/td><\/tr>
    F1<\/td>1<\/td>Conversion factor<\/td><\/tr>
    F2<\/td>1<\/td>Conversion factor<\/td><\/tr><\/tbody><\/table>

    <\/p>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t<\/div>\n\t\t","protected":false},"excerpt":{"rendered":"

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